Advanced Package Preview
Illustrative configuration
This example illustrates an advanced package structure: results, QC, calibration, and representative instrument artifacts — instrument logs, data sheets, chromatograms, spectra, extraction logs, digestion logs, and instrument sequences.
Package
CLE-2026-SDG-0142_demo-package.zip · locally generated demo fixtureSDG
CLE-2026-SDG-0142
Lab
Demo Environmental Laboratory · DEMO-CERT-001
Generated
2026-06-16 14:32 by kpatel
Configuration
Package contents and validation are mapped to the laboratory’s approved requirements
Package contents
| Folder / File | Type | Size | Files | |
|---|---|---|---|---|
| 01_CaseNarrative/ | Case narrative + cover letter | 184 KB | 2 | |
| 02_AnalyticalResults/ | Form I-IN per sample | 312 KB | 5 | |
| 03_ChainOfCustody/ | Signed COC PDFs | 2.4 MB | 3 | |
| 04_QCSummaries/ | MB, LCS/LCSD, MS/MSD, Duplicates | 608 KB | 14 | |
| 05_Calibration/ | ICAL, CCV, ICB/CCB, ICS | 1.2 MB | 21 | |
| 06_InstrumentTune/ | ICP-MS tune reports | 96 KB | 3 | |
| 07_RawData/ | Instrument output, logs, sequences | 42.1 MB | 178 | |
| 07_RawData/Sequences/seq_20260616_run01.csv | Instrument run sequence | 4.2 KB | — | |
| 07_RawData/ICPMS/GW-0010_raw.csv | Raw counts/intensity | 148 KB | — | |
| 07_RawData/ICPMS/GW-0010_dil10_raw.csv | Raw counts/intensity (×10 dilution re-run) | 148 KB | — | |
| 07_RawData/Chromatograms/GW-0010_Zn.png | Mass spectrum (⁶⁴Zn / ⁶⁶Zn isotopes) | 284 KB | — | |
| 07_RawData/Logs/digestion_log_20260615.pdf | EPA 3005A digestion log (scanned) | 1.8 MB | — | |
| 07_RawData/Logs/instrument_log_ICPMS01_20260616.pdf | Instrument operations log | 620 KB | — | |
| 07_RawData/Extraction/extraction_batch_20260615.csv | Sample prep tracking | 8.4 KB | — | |
| ... 172 additional raw data files ... | ||||
| 08_Signatures/ | Approver signatures + audit log | 72 KB | 4 | |
Sample raw data — Zn original vs. ×10 dilution
GW-0010 Original Run — ⁶⁶Zn intensity
Mass: 66 Zn
Counts: 64,852,140 cps
Cal range: 0–5000 µg/L = 0–62,485,200 cps
Predicted: ~5,200 µg/L (extrapolated)
⚠ Result exceeds ICAL-5 (high std)
Flag: E — reanalysis required
Internal std (⁶Li): 1,240,800 cps (stable)
Tune drift: -0.4% (within spec)
Counts: 64,852,140 cps
Cal range: 0–5000 µg/L = 0–62,485,200 cps
Predicted: ~5,200 µg/L (extrapolated)
⚠ Result exceeds ICAL-5 (high std)
Flag: E — reanalysis required
Internal std (⁶Li): 1,240,800 cps (stable)
Tune drift: -0.4% (within spec)
GW-0010 ×10 Dilution Re-run — ⁶⁶Zn intensity
Mass: 66 Zn
Counts: 15,494,896 cps
Dilution factor: ×10
Diluted result: 1,240 µg/L
Final: 12,400 µg/L ✓
Flag: D — reportable
Internal std (⁶Li): 1,241,200 cps (stable)
Tune drift: -0.5% (within spec)
Counts: 15,494,896 cps
Dilution factor: ×10
Diluted result: 1,240 µg/L
Final: 12,400 µg/L ✓
Flag: D — reportable
Internal std (⁶Li): 1,241,200 cps (stable)
Tune drift: -0.5% (within spec)